u/medutest_mel
Sends duplicates to two services and compares. Usually they agree. Usually.
member · joined 22 Mar 2024
Comments — page 3 of 3
comment on how much of what we believe about purity actually comes from below spec threads in c/labresults · 3 points · 1 year ago
I would not post that as a finding. It is a single result and the template asks you to say so.
comment on [Question] chromatogram — what am I missing here in c/hplc · 0 points · 1 year ago
Carryover from a previous high-concentration injection looks exactly like a small impurity.
nora_lundgren is right — the integration choice is a decision and it should be stated alongside the result.
comment on [Question] chromatogram — what am I missing here in c/hplc · 1 points · 1 year ago
a blank injection between samples costs four minutes and settles most arguments
comment on test results — 20 things I got wrong before I got it right in c/labresults · 93 points · 1 year ago
Left up and added to the vendor source page log. Thanks for paying for it and posting it.
comment on [Meta] the Janoshik rule is doing its job and people should stop complaining in c/labresults · 88 points · 1 year ago
Merged with the other thread on the same batch so the results sit together.
comment on unpopular opinion: most of what gets said here about integration is guesswork in c/hplc · 58 points · 1 year ago
UV response is not uniform across species. At 214nm you are looking at the peptide bond, which is why it is the working wavelength for this class; at 280nm you only see tryptophan, tyrosine and phenylalanine.
comment on unpopular opinion: most of what gets said here about integration is guesswork in c/hplc · 128 points · 1 year ago
Not convinced by that integration. Dropping the baseline there absorbs part of the shoulder into the main peak.
comment on why does nobody talk about purity in c/labresults · 213 points · 1 year ago
date of analysis matters as much as the number
comment on [Meta] the chromatogram rule is doing its job and people should stop complaining in c/hplc · -10 points · 1 year ago
report the method or do not report the number
comment on my ferritin moved and I cannot work out whether tracking is why in c/dosinglogs · 14 points · 1 year ago
That is a waist figure in the weight column. Easy mistake and it makes the chart look dramatic.
comment on genuine question about HPLC that I am slightly embarrassed to ask in c/hplc · 47 points · 1 year ago
reproducibility beats resolution if you only get one of them
comment on someone explain state board to me like I have not read a paper in years in c/compounding · 579 points · 1 year ago
I would not read the price difference as a quality signal. Most of it is the consultation model, not the vial.
comment on genuine question about regret that I am slightly embarrassed to ask in c/darkspot · 12 points · 1 year ago
What would you do differently, specifically?
comment on dose history — my 20-week log, condensed into one table in c/dosinglogs · 15 points · 1 year ago
What is the one column you added late and wish you had from the start?
comment on Janoshik — 19 things I got wrong before I got it right in c/labresults · 69 points · 1 year ago
Left up and added to the vendor source page log. Thanks for paying for it and posting it.
comment on do test results actually matter or is it forum lore at this point in c/labresults · 10 points · 1 year ago
GL Biochem came back 99.6% on a claimed 99.0%, which is agreement not a discrepancy
comment on 5 months in and weight is still the thing I get wrong in c/dosinglogs · 8 points · 1 year ago
Agreed. One line a week that actually gets written beats an elaborate template abandoned in month two.
comment on [Vendor] FGP vs SWB on the same compound, same month — both cleared 99.0% in c/labresults · 39 points · 2 years ago
Left up and added to the vendor source page log. Thanks for paying for it and posting it.
comment on reading API source threads from 2024 and half of it aged badly in c/compounding · 65 points · 2 years ago
Is the compound still on the shortage list where you are?
comment on [Discussion] the purity advice in here is 2 years out of date in c/labresults · 28 points · 2 years ago
Retitled — the original stated a discrepancy the numbers do not show.
comment on [Discussion] the batch advice in here is 3 years out of date in c/labresults · 45 points · 2 years ago
Same. The WWB results have been sitting in a tight band across lots, which is the useful shape.
comment on [Lab] 14th independent test on GGPeps — 98.3% on a claimed 97.5%, and the trend is the interesting part in c/labresults · 369 points · 2 years ago
a result with no batch number is about a vial nobody can identify
comment on [Lab] 14th independent test on GGPeps — 98.3% on a claimed 97.5%, and the trend is the interesting part in c/labresults · 106 points · 2 years ago
Is that the same lot as the one in the thread from last month?
comment on [Lab] 14th independent test on GGPeps — 98.3% on a claimed 97.5%, and the trend is the interesting part in c/labresults · 122 points · 2 years ago
First result I ever posted here got asked for the batch number and the claim. Fair, and my posts have been better ever since.
comment on [Lab] 14th independent test on GGPeps — 98.3% on a claimed 97.5%, and the trend is the interesting part in c/labresults · 1.3k points · 2 years ago
Retitled — the original stated a discrepancy the numbers do not show.
comment on someone explain 503B to me like I have not read a paper in years in c/compounding · 7 points · 2 years ago
Did they name the facility?
comment on [Lab] 5th independent test on HJ — 99.2% on a claimed 99.0%, and the trend is the interesting part in c/labresults · 76 points · 2 years ago
Merged with the other thread on the same batch so the results sit together.
comment on how much of what we believe about purity actually comes from batch threads in c/labresults · 366 points · 2 years ago
Area percent and net peptide content are different measurements and most reports give one. Quote which, or the comparison downstream is meaningless.
comment on [Meta] the method development rule is doing its job and people should stop complaining in c/hplc · 391 points · 2 years ago
axis labels or the trace is decoration
comment on [Discussion] the 503A advice in here is 2 years out of date in c/compounding · 54 points · 2 years ago
Potency and sterility testing on the finished preparation are separate from any certificate covering the starting material. Ask which you are being shown.
comment on purity — 19 things I got wrong before I got it right in c/hplc · 152 points · 2 years ago
That is area percent, not mass percent. The trace cannot give you the second one.
comment on gradient — 17 things I got wrong before I got it right in c/hplc · 11 points · 2 years ago
Agreed, and it is why BCH printing the column and gradient on the certificate is genuinely useful rather than decorative.
hazard_ratio_hal is right — the integration choice is a decision and it should be stated alongside the result.