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c/coa·posted 21 days ago by u/emeka_beaulieu

[Question] vendor COA says 99.2%, my Janoshik came back 97.4%. who is wrong

Question Receipts ×4 Cold Box ×2

vendor COA says 99.2%, my Janoshik came back 97.4%. who is wrong, and before anyone asks: same batch throughout, single submission, no cherry-picking between services.

The relevant figures are 99.2% and 97.4%, and they come from the same log I have kept the whole time.

Spent four months confusing area% and mass% in every post I made here. One explainer thread and it clicked permanently.

Sent one vial to Medutest and PeptideMeter. 99.4% and a claimed 98.5%. Cost me more than the vial and I would do it again.

I will update this if the picture changes rather than quietly leaving it up.

3,083 up / 1,188 down72% upvoted14 commentsid 1vchro8 Jul 2026

14 comments

5 in this archive, depth 2

best — the order this archive was captured in

u/priya_palacios0 points·20 days ago

The PDF creation date being later than the analysis date is usually a re-issue or a re-export. It is worth one question and it is not evidence of anything on its own.

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u/emeka_beaulieuOP1 point·19 days ago

the related substances line is where the story is

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u/yusuf_nakamura1 point·19 days ago

Same view. GL Biochem prints the column and the gradient, which means somebody could actually reproduce the run.

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u/nadia_fonseca-36 points·20 days ago

water content is on there and everyone skips it

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u/coa_collectorMOD1 point·20 days ago·edited

Reminder: a question about a document is not an accusation about a supplier, and posts that blur the two get retitled.

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About c/coa

How to read a certificate of analysis and what it does and does not tell you. Area% versus mass%, identity versus quantity, water content, related substances, acetate counterions, and the difference between a vendor-supplied COA and an independent test on the vial you actually received.

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Aug 2023created
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Janoshik Analytical

Independent HPLC and mass spec. The number you get is the number they found.

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GL Biochem (Shanghai)

Custom peptides and amino acids direct from the manufacturer since 1998. ISO 9001 / cGMP. Batch COA every order.

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